The Zurich group first split each ultrasonically cleaned sample in half, with the treatment of the second set of samples being deferred until the radiocarbon measurements on the first set had been completed.
The first set of samples was further subdivided into three portions.
Even for the first investigation, there was a possibility of using radiocarbon dating to determine the age of the linen from which the shroud was woven.
The size of the sample then required, however, was ~500cm, which would clearly have resulted in an unacceptable amount of damage, and it was not until the development in the 1970s of small gas-counters and accelerator-mass-spectrometry techniques (AMS), requiring samples of only a few square centimetres, that radiocarbon dating of the shroud became a real possibility. The shroud was separated from the backing cloth along its bottom left-hand edge and a strip (~10 mm x 70 mm) was cut from just above the place where a sample was previously removed in 1973 for examination.
On the basis of the stylistic details and the historical evidence the cope could be dated at ~ AD 1290 - 1310 (reign of King Phillipe IV).
Because it was not known to what degree dirt, smoke or other contaminants might affect the linen samples, all three laboratories subdivided the samples, and subjected the pieces to several different mechanical and chemical cleaning procedures.
Among those present when the sample as cut from the shroud were Cardinal Anastasio Ballestrero (Archbishop of Turin), Professor L. The laboratories were not told which container held the shroud sample.
Gonella (Department of Physics, Turin Polytechnic and the Archbishop's scientific adviser), two textile experts (Professor F. Because the distinctive three-to-one herringbone twill weave of the shroud could not be matched in the controls, however, it was possible for a laboratory to identify the shroud sample.1 - Department of Geosciences, 2 - Department of Physics, University of Arizona, Tucson, Arizona 85721, USA 3 - Research Laboratory for Archaeology and History of Art, University of Oxford, Oxford, OX1 3QJ, UK 4 - Institut für Mittelenergiephysik, ETH-Hönggerberg, CH-8093 Zürich, Switzerland 5 - Lamont-Doherty Geological Observatory, Columbia University, Palisades, New York 10964, USA 6 - Research Laboratory, British Museum, London WC1B 3DG, UK Very small samples from the Shroud of Turin have been dated by accelerator mass spectrometry in laboratories at Arizona, Oxford and Zurich.As Controls, three samples whose ages had been determined independently were also dated.Testore of Department of Materials Science, Turin Polytechnic and G. If the samples had been unravelled or shredded rather than being given to the laboratories as whole pieces of cloth, then it would have been much more difficult, but not impossible, to distinguish the shroud sample from the controls.Vial of Musée des Tissues and Centre International d'Étude des Textiles Anciens in Lyon), Dr M. Tite of the British Museum, representatives of the three radiocarbon-dating laboratories (Professor P. (With unravelled or shredded samples, pretreatment cleaning would have been more difficult and wasteful.) Because the shroud had been exposed to a wide range of potential sources of contamination and because of the uniqueness of the samples available, it was decided to abandon blind-test procedures in the interests of effective sample pretreatment.To confirm the feasibility of dating the shroud by these methods an intercomparison, involving four AMS and two small gas-counter radiocarbon laboratories and the dating of three known-age textile samples, was coordinated by the British Museum in 1983. The strip came from a single site on the main body of the shroud away from any patches or charred areas.